3LOT
Crystal structure of PROTEIN OF UNKNOWN FUNCTION (NP_070038.1) from ARCHAEOGLOBUS FULGIDUS at 1.89 A resolution
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-05-14 |
Detector | MARMOSAIC 325 mm CCD |
Wavelength(s) | 0.91162,0.97936,0.97922 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 75.786, 103.079, 156.550 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.970 - 1.890 |
R-factor | 0.159 |
Rwork | 0.156 |
R-free | 0.20600 |
Structure solution method | MAD |
RMSD bond length | 0.018 |
RMSD bond angle | 1.537 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SHELX |
Refinement software | REFMAC (5.5.0053) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 48.970 | 48.970 | 1.960 |
High resolution limit [Å] | 1.890 | 4.060 | 1.890 |
Rmerge | 0.107 | 0.040 | 0.552 |
Number of reflections | 98016 | 10168 | 9838 |
<I/σ(I)> | 9.84 | 26.6 | 2.2 |
Completeness [%] | 99.2 | 97.3 | 97.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.6 | 277 | 0.2000M ammonium acetate, 30.0000% polyethylene glycol 4000, 0.1M sodium citrate pH 5.6, NANODROP', VAPOR DIFFUSION, SITTING DROP, temperature 277K |