3L8L
Gramicidin D complex with sodium iodide
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 5ID-B |
Synchrotron site | APS |
Beamline | 5ID-B |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2000 |
Detector | MAR CCD 165 mm |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 29.816, 31.255, 51.667 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 26.740 - 1.250 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1w5u |
RMSD bond length | 0.015 |
RMSD bond angle | 0.035 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | SHELXL-97 |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 26.740 |
High resolution limit [Å] | 1.250 |
Number of reflections | 19883 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | BATCH CRYSTALLIZATION WITH 30 MG/ML GRAMICIDIN AND SATURATED NAI IN METHANOL |