Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.1 |
Synchrotron site | ALS |
Beamline | 5.0.1 |
Detector technology | CCD |
Detector | ADSC QUANTUM 210 |
Spacegroup name | H 3 2 |
Unit cell lengths | 76.810, 76.810, 85.900 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 30.000 - 2.200 |
R-factor | 0.23 |
Rwork | 0.230 |
R-free | 0.26900 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.004 |
RMSD bond angle | 1.320 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | CNS (1.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.280 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.085 | 0.414 |
Number of reflections | 4836 | |
Completeness [%] | 95.0 | 69.1 |
Redundancy | 8.8 | 2.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 30% PEG 200, 50MM CACL2, 100MM HEPES-KOH PH 7.0, VAPOR DIFFUSION, HANGING DROP, TEMPERATURE 296K |