3JZG
Structure of EED in complex with H3K27me3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E+ DW |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2009-08-01 |
Detector | RIGAKU RAXIS |
Wavelength(s) | 1.54 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 57.775, 85.263, 91.169 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 62.270 - 2.100 |
R-factor | 0.16107 |
Rwork | 0.158 |
R-free | 0.22177 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.023 |
RMSD bond angle | 1.931 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0072) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 62.300 |
High resolution limit [Å] | 2.100 |
Rmerge | 0.144 |
Number of reflections | 26778 |
<I/σ(I)> | 5.1 |
Completeness [%] | 99.0 |
Redundancy | 5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 300 | 3.5M NaF, pH 7.5, VAPOR DIFFUSION, SITTING DROP, temperature 300K |