3HMK
Crystal Structure of Serine Racemase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-09-17 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.0332 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 48.261, 102.960, 120.923 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.100 - 2.100 |
R-factor | 0.24389 |
Rwork | 0.241 |
R-free | 0.28949 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1fkp |
RMSD bond length | 0.007 |
RMSD bond angle | 0.993 |
Data reduction software | CrystalClear |
Data scaling software | CrystalClear |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0072) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.100 | 2.180 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.069 | 0.195 |
Number of reflections | 32657 | |
<I/σ(I)> | 10.1 | 3.5 |
Completeness [%] | 95.8 | 74.8 |
Redundancy | 3.17 | 1.95 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | pH 8.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |