3GV8
Human DNA polymerase iota in complex with T template DNA and incoming dGTP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Collection date | 2008-03-07 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 98.070, 98.070, 203.380 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 23.840 - 2.000 |
R-factor | 0.219 |
Rwork | 0.218 |
R-free | 0.24800 |
RMSD bond length | 0.019 |
RMSD bond angle | 1.821 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.070 |
High resolution limit [Å] | 2.000 | 4.310 | 2.000 |
Rmerge | 0.121 | 0.083 | 0.577 |
Number of reflections | 40059 | ||
<I/σ(I)> | 57.94 | ||
Completeness [%] | 99.7 | 97.1 | 100 |
Redundancy | 13.3 | 12.7 | 8.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | hanging drop | 6.5 | 15% PEG 5000MME, 0.2M NH4SO4, 0.1M MES 6.5, 5% glycerol, hanging drop |