3F7S
CRYSTAL STRUCTURE OF A NTF2-LIKE PROTEIN OF UNKNOWN FUNCTION (PP_4556) FROM PSEUDOMONAS PUTIDA KT2440 AT 2.11 A RESOLUTION
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-B |
Synchrotron site | APS |
Beamline | 23-ID-B |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-10-13 |
Detector | MARMOSAIC 300 mm CCD |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 65.920, 65.920, 89.390 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.476 - 2.110 |
R-factor | 0.179 |
Rwork | 0.177 |
R-free | 0.21700 |
Structure solution method | SAD |
RMSD bond length | 0.016 |
RMSD bond angle | 1.517 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SHELX |
Refinement software | REFMAC (5.5.0053) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 29.476 | 29.476 | 2.190 |
High resolution limit [Å] | 2.110 | 4.530 | 2.110 |
Rmerge | 0.120 | 0.041 | 0.986 |
Number of reflections | 11917 | 2204 | 2296 |
<I/σ(I)> | 9.68 | 28.2 | 1.6 |
Completeness [%] | 99.9 | 99.5 | 99.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 10.5 | 277 | 0.8000M K2HPO4, 0.2000M Li2SO4, 1.2000M NaH2PO4, 0.1M CAPS pH 10.5, NANODROP, VAPOR DIFFUSION, SITTING DROP, temperature 277K |