3CG1
Crystal structure of P. furiosus periplasmic binding protein ModA/WtpA with bound tungstate
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2007-09-16 |
| Detector | PSI PILATUS 6M |
| Wavelength(s) | 1.21340 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 46.460, 109.790, 55.430 |
| Unit cell angles | 90.00, 96.22, 90.00 |
Refinement procedure
| Resolution | 30.000 - 1.600 |
| Rwork | 0.186 |
| R-free | 0.20460 |
| Structure solution method | SAD |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.700 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | CNS |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | |
| High resolution limit [Å] | 1.600 | 1.600 |
| Number of reflections | 140430 | |
| Completeness [%] | 97.7 | 93.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 9 | 293 | Bicine, NaCl, PEG 600, pH 9.0, VAPOR DIFFUSION, SITTING DROP, temperature 293K |
