3BZL
Crystal structural of native EscU C-terminal domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL11-1 |
Synchrotron site | SSRL |
Beamline | BL11-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-11-30 |
Detector | MARMOSAIC 325 mm CCD |
Wavelength(s) | 0.97945 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 102.424, 55.121, 50.257 |
Unit cell angles | 90.00, 110.42, 90.00 |
Refinement procedure
Resolution | 30.000 - 1.710 |
R-factor | 0.188 |
Rwork | 0.187 |
R-free | 0.21700 |
Structure solution method | SIRAS |
RMSD bond length | 0.012 |
RMSD bond angle | 1.380 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SHELX |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.780 |
High resolution limit [Å] | 1.710 | 3.710 | 1.710 |
Rmerge | 0.056 | 0.042 | 0.355 |
Number of reflections | 27830 | ||
<I/σ(I)> | 19.9 | ||
Completeness [%] | 98.5 | 96.7 | 90.4 |
Redundancy | 5.8 | 5.2 | 5.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 8 | 293 | NaFormate, NaCl, Tris, pH 8.0, VAPOR DIFFUSION, temperature 293K |