3AG4

Bovine Heart Cytochrome c Oxidase in the Cyanide Ion-bound Fully Reduced State at 100 K

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL44XU
Synchrotron site	SPring-8
Beamline	BL44XU
Temperature [K]	100
Collection date	2002-07-07
Wavelength(s)	0.9
Spacegroup name	P 21 21 21
Unit cell lengths	183.364, 206.648, 178.137
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	40.000 - 2.050
Rwork	0.186
R-free	0.21900
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2eij
Data reduction software	DENZO
Data scaling software	SCALEPACK
Refinement software	REFMAC (5.3)

Data quality characteristics

	Overall
Low resolution limit [Å]	52.600
High resolution limit [Å]	2.050
Number of reflections	430029

Crystallization Conditions

crystal ID	method	pH	temperature	details
1