2XVW
Human serum albumin complexed with dansyl-L-arginine and myristic acid
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE X11 |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | X11 |
Temperature [K] | 298 |
Detector technology | CCD |
Collection date | 2001-12-04 |
Detector | MARRESEARCH |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 187.080, 38.760, 95.730 |
Unit cell angles | 90.00, 105.64, 90.00 |
Refinement procedure
Resolution | 32.570 - 2.650 |
R-factor | 0.191 |
Rwork | 0.191 |
R-free | 0.25200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1e7g |
RMSD bond length | 0.007 |
RMSD bond angle | 1.200 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | CNS |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 32.600 | 2.820 |
High resolution limit [Å] | 2.650 | 2.650 |
Rmerge | 0.060 | 0.400 |
Number of reflections | 19137 | |
<I/σ(I)> | 10.6 | 2.8 |
Completeness [%] | 97.4 | 99 |
Redundancy | 2.7 | 2.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | SEE PAPER, pH 7 |