2X9H
CRYSTAL STRUCTURE OF MYOSIN-2 MOTOR DOMAIN IN COMPLEX WITH ADP- METAVANADATE AND PENTACHLOROCARBAZOLE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 77 |
Detector technology | CCD |
Collection date | 2010-02-24 |
Detector | ADSC CCD |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 89.160, 146.630, 153.680 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.770 - 2.700 |
R-factor | 0.20751 |
Rwork | 0.203 |
R-free | 0.28871 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2jhr |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | ARP (WARP CNS REFMAC) |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.770 | 2.769 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.400 | |
Number of reflections | 26158 | |
<I/σ(I)> | 2.4 | |
Completeness [%] | 100.0 | 100 |
Redundancy | 5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.4 | 50 MM TRIS-HCL PH 7.4, 140 MM NACL, 9% W/V PEG8000, 2% (V/V) MPD, 5 MM MGCL2, 5 MM DTT, 1 MM EGTA |