2VKP
Crystal structure of BTB domain from BTBD6
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2007-10-26 |
| Detector | MARRESEARCH |
| Wavelength(s) | 0.98248, 0.97874 |
| Spacegroup name | P 65 2 2 |
| Unit cell lengths | 58.135, 58.135, 332.456 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 43.070 - 1.900 |
| R-factor | 0.196 |
| Rwork | 0.194 |
| R-free | 0.23400 |
| Structure solution method | SAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.016 |
| RMSD bond angle | 1.361 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | SHELXDE |
| Refinement software | REFMAC (5.4.0066) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.000 |
| High resolution limit [Å] | 1.900 | 1.900 |
| Rmerge | 0.090 | 0.860 |
| Number of reflections | 27754 | |
| <I/σ(I)> | 15.8 | 3.8 |
| Completeness [%] | 99.9 | 100 |
| Redundancy | 6.4 | 6.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 6.5 | 0.8M POTASSIUM CITRATE, 0.1M SODIUM CACODYLATE PH6.5 |
