2VC0
Feast or famine regulatory protein (Rv3291c)from M. tuberculosis complexed with L-Leucine
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Temperature [K] | 298 |
| Spacegroup name | P 42 21 2 |
| Unit cell lengths | 100.875, 100.875, 99.271 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 71.250 - 2.500 |
| R-factor | 0.214 |
| Rwork | 0.212 |
| R-free | 0.25700 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 2.650 |
| High resolution limit [Å] | 2.500 | 2.500 |
| Rmerge | 0.095 | 0.520 |
| Number of reflections | 64899 | |
| <I/σ(I)> | 11 | 2.3 |
| Completeness [%] | 96.0 | 98.3 |
| Redundancy | 3.7 | 3.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 295 |
