2V65
Apo LDH from the psychrophile C. gunnari
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM30A |
Synchrotron site | ESRF |
Beamline | BM30A |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MARRESEARCH |
Spacegroup name | C 2 2 2 |
Unit cell lengths | 113.790, 113.790, 109.900 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.790 - 2.350 |
R-factor | 0.228 |
Rwork | 0.228 |
R-free | 0.24100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1v6a |
RMSD bond length | 0.013 |
RMSD bond angle | 1.400 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.400 |
High resolution limit [Å] | 2.350 | 2.350 |
Rmerge | 0.100 | 0.210 |
Number of reflections | 28796 | |
<I/σ(I)> | 9.51 | 5.08 |
Completeness [%] | 95.9 | 97.1 |
Redundancy | 2.97 | 3.09 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.8 | 277 | 0.1M HEPES PH 7.8, 0.2M PROLINE, 14% PEG 3350, 4 DEG C |