2V3O
Thrombin with 3-cycle with F
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | ENRAF-NONIUS FR571 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 1999-11-15 |
| Detector | MARRESEARCH |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 70.610, 71.820, 72.280 |
| Unit cell angles | 90.00, 100.60, 90.00 |
Refinement procedure
| Resolution | 71.070 - 1.790 |
| R-factor | 0.178 |
| Rwork | 0.176 |
| R-free | 0.21200 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.437 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | CCP4 |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.900 |
| High resolution limit [Å] | 1.790 | 1.790 |
| Rmerge | 0.080 | 0.330 |
| Number of reflections | 29953 | |
| <I/σ(I)> | 25.6 | 8.3 |
| Completeness [%] | 87.5 | 78.7 |
| Redundancy | 2.58 | 2.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
