2RER
Crystal structure of the aromatase/cyclase domain of TcmN from Streptomyces glaucescens
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-12-04 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97957 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 69.660, 105.126, 50.259 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 31.310 - 1.900 |
Rwork | 0.215 |
R-free | 0.24900 |
Structure solution method | MAD |
RMSD bond length | 0.006 |
RMSD bond angle | 1.100 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.940 |
High resolution limit [Å] | 1.900 | 1.900 |
Number of reflections | 14977 | |
<I/σ(I)> | 16.9 | 3.4 |
Completeness [%] | 99.8 | 98.2 |
Redundancy | 7 | 5.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.6 | 277 | 24% PEG 8000, 0.1M SODIUM ACETATE, pH 4.60, VAPOR DIFFUSION, SITTING DROP, temperature 277K |
1 | VAPOR DIFFUSION, SITTING DROP | 4.6 | 277 | 24% PEG 8000, 0.1M SODIUM ACETATE, pH 4.60, VAPOR DIFFUSION, SITTING DROP, temperature 277K |