2QDK
X-ray structure of the unliganded uridine phosphorylase from Salmonella typhimurium at 1.62A resolution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE X11 |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | X11 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MAR CCD 165 mm |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 89.600, 125.030, 134.950 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 6.000 - 1.620 |
Rwork | 0.191 |
Structure solution method | MOLECULAR REPLACEMENT |
Refinement software | PHENIX |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 25.400 |
High resolution limit [Å] | 1.600 |
Number of reflections | 187456 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 297 | VAPOR DIFFUSION, HANGING DROP, temperature 297K |