2Q7J
The Wild Type Androgen Receptor Ligand Binding Domain Bound with Testosterone and a TIF2 box 3 Coactivator Peptide 740-753
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-BM |
Synchrotron site | APS |
Beamline | 17-BM |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-04-01 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 54.779, 66.871, 70.237 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.550 - 1.900 |
R-factor | 0.18153 |
Rwork | 0.180 |
R-free | 0.22027 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.133 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.550 | 1.970 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.440 | 0.526 |
Number of reflections | 20209 | |
<I/σ(I)> | 47.4 | 3.8 |
Completeness [%] | 99.9 | 100 |
Redundancy | 7.2 | 6.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |