Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | SIEMENS |
Temperature [K] | 298 |
Collection date | 1994-08-26 |
Detector | SIEMENS |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 128.500, 128.500, 116.300 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.170 - 2.300 |
R-factor | 0.173 * |
Rwork | 0.192 |
R-free | 0.24600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2prj |
RMSD bond length | 0.016 * |
RMSD bond angle | 3.100 * |
Data reduction software | XDS |
Refinement software | X-PLOR (3.851) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.170 | 2.400 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.065 | |
Total number of observations | 75440 * | |
Number of reflections | 41448 | |
<I/σ(I)> | 12 | |
Completeness [%] | 94.7 | 76.8 |
Redundancy | 1.82 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.7 | 293 | Oikonomakos, N.G., (1985) Biochim. Biophys. Acta, 832, 248. * |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | DITHIOTHREITOL | ||
2 | 1 | 1 | BES | ||
3 | 1 | 1 | EDTA | ||
4 | 1 | 1 | NAN3 |