2PEI
Crystal structure of selenomethionine-labeled RbcX
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-07-01 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.97950 |
Spacegroup name | P 1 |
Unit cell lengths | 70.362, 71.102, 113.162 |
Unit cell angles | 89.58, 81.10, 80.09 |
Refinement procedure
Resolution | 20.000 - 2.700 |
R-factor | 0.215 |
Rwork | 0.212 |
R-free | 0.26200 |
Structure solution method | SAD |
RMSD bond length | 0.020 |
RMSD bond angle | 1.683 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SHARP |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 111.803 | 68.520 | 2.850 |
High resolution limit [Å] | 2.700 | 8.540 | 2.700 |
Rmerge | 0.101 | 0.043 | 0.420 |
Total number of observations | 6640 | 31838 | |
Number of reflections | 56794 | ||
<I/σ(I)> | 6.2 | 12.9 | 1.5 |
Completeness [%] | 96.9 | 97.4 | 96.3 |
Redundancy | 3.9 | 3.7 | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 293 | 30% PEG 4000, 0.1 M Tris-HCl pH 8.5, 0.2 M Sodium acetate, VAPOR DIFFUSION, HANGING DROP, temperature 293K |