2P28
Structure of the PHE2 and PHE3 fragments of the integrin beta2 subunit
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-09-25 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.976 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 52.260, 52.260, 423.924 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | 2.257 |
High resolution limit [Å] | 2.200 | 2.200 |
Number of reflections | 18866 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | 0.2M ammonium sulphate, 15% PEG4000, 5% isopropanol, VAPOR DIFFUSION, HANGING DROP, temperature 291K |