2OSV
Crystal Structure of ZnuA from E. coli
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X4A |
Synchrotron site | NSLS |
Beamline | X4A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-07-11 |
Detector | ADSC QUANTUM 4 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 72.980, 87.985, 86.728 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 1.750 |
Rwork | 0.175 |
R-free | 0.21600 |
Structure solution method | SAD |
RMSD bond length | 0.012 |
RMSD bond angle | 1.273 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SOLVE (2.11) |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.795 |
High resolution limit [Å] | 1.750 | 1.750 |
Rmerge | 0.085 | 0.442 |
Number of reflections | 56935 | |
<I/σ(I)> | 19.3 | 3.9 |
Completeness [%] | 99.9 | 99.8 |
Redundancy | 5.1 | 4.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5 | 293 | 100mM sodium acetate, 25% PEG 3350, pH 5.0, VAPOR DIFFUSION, SITTING DROP, temperature 293K |