2LU4

Solution NMR structure of the beta2 carbohydrate module of AMP-activated protein kinase bound to glucosyl-cyclodextrin

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	AVANCE	Bruker Avance	800
2	Bruker	AVANCE	Bruker Avance	600

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	2	3D CBCA(CO)NH
10	1	1	3D 1H-15N NOESY
11	1	4	3D 1H-13C NOESY aliphatic
12	1	1	3D HNHA
13	1	1	3D HNHB
14	1	4	3D HACAHB-COSY
15	1	1	2D 1H-15N HSQC
16	1	4	3D13C,15N-filtered,edited NOESY
2	1	2	3D HNCACB
3	1	2	3D HNCO
4	1	2	3D HBHA(CO)NH
5	1	2	3D H(CCO)NH
6	1	2	3D C(CO)NH
7	1	4	3D HCCH-TOCSY
8	1	3	2D 1H-1H TOCSY
9	1	3	2D 1H-1H NOESY

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	6.9	ambient	298

Conformers

Conformers Calculated Total Number	100
Conformers Submitted Total Number	20