2JKJ
DraE Adhesin in complex with Chloramphenicol Succinate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | BRUKER AXS MICROSTAR |
Temperature [K] | 100 |
Collection date | 2004-12-14 |
Detector | BRUKER |
Spacegroup name | P 3 |
Unit cell lengths | 119.600, 119.600, 57.700 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 25.000 - 2.300 |
R-factor | 0.25 |
Rwork | 0.249 |
R-free | 0.27800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1usq |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | BUSTER-TNT |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | 2.400 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.100 | 0.330 |
Number of reflections | 43763 | |
<I/σ(I)> | 8.9 | 2.2 |
Completeness [%] | 100.0 | 99.9 |
Redundancy | 4.3 | 4.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 2M AMMONIUM SULPHATE, 0.1-20 MM CHLORAMPHENICOL SUCCINATE, 0.1 M HEPES PH 7.0 SOAKED IN SATURATED THIAMPHENICOL SOLUTION |