2J0A
Structure of the catalytic domain of mouse Manic Fringe
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-3 |
Synchrotron site | ESRF |
Beamline | ID14-3 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-05-30 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 162.600, 41.400, 39.800 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 81.380 - 1.800 |
R-factor | 0.195 |
Rwork | 0.194 |
R-free | 0.21900 |
Structure solution method | SAD |
RMSD bond length | 0.019 |
RMSD bond angle | 1.739 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 81.400 | 1.900 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.060 | 0.440 |
Number of reflections | 25066 | |
<I/σ(I)> | 13.2 | 2.9 |
Completeness [%] | 99.5 | 97.9 |
Redundancy | 4.4 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | 0.2 M POTASSIUM SULFATE, 20% PEG 3350, pH 6.50 |