2IOM
Mouse p53 core domain soaked with 2-propanol
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 92.2 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS IV |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 92.299, 44.541, 62.915 |
Unit cell angles | 90.00, 126.23, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.000 |
R-factor | 0.209 |
Rwork | 0.209 |
R-free | 0.24600 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.440 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.063 | 0.263 |
Number of reflections | 57269 | |
<I/σ(I)> | 21.1 | 3.92 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 293 | 100mM Tris, 16-18% PEG 2K MME, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K, pH 7.00 |