2HPD
CRYSTAL STRUCTURE OF HEMOPROTEIN DOMAIN OF P450BM-3, A PROTOTYPE FOR MICROSOMAL P450'S
Experimental procedure
Spacegroup name | P 1 21 1 |
Unit cell lengths | 59.400, 154.000, 62.200 |
Unit cell angles | 90.00, 94.70, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.000 |
R-factor | 0.167 |
Rwork | 0.167 |
RMSD bond length | 0.016 |
RMSD bond angle | 3.100 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.000 * |
Rmerge | 0.058 * |
Total number of observations | 251913 * |
Number of reflections | 55129 * |
Completeness [%] | 73.6 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 5 (mM) | about 275mg/ml |
2 | 1 | drop | potassium phosphate | 50 (mM) | |
3 | 1 | reservoir | PIPES | 100 (mM) | |
4 | 1 | reservoir | PEG8000 | 20 (%(w/v)) | |
5 | 1 | reservoir | dithiothreitol | 15 (mM) | |
6 | 1 | reservoir | 40 (mM) |