2HP1
Inter-subunit signaling in GSAM
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE BW7B |
Synchrotron site | EMBL/DESY, Hamburg |
Beamline | BW7B |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Detector | MAR scanner 180 mm plate |
Wavelength(s) | 0.909 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 66.483, 106.981, 119.499 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 22.520 - 2.080 |
R-factor | 0.201 |
Rwork | 0.201 |
R-free | 0.25400 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.300 |
Data reduction software | MOSFLM |
Data scaling software | CCP4 ((SCALA)) |
Phasing software | AMoRE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 23.000 |
High resolution limit [Å] | 2.080 |
Number of reflections | 47046 |
Completeness [%] | 90.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.2 | 292 | pH 7.2, VAPOR DIFFUSION, temperature 292K |