Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX II BEAMLINE I711 |
Synchrotron site | MAX II |
Beamline | I711 |
Temperature [K] | 278 |
Detector technology | IMAGE PLATE |
Collection date | 1999-12-07 |
Detector | MARRESEARCH |
Spacegroup name | H 3 2 |
Unit cell lengths | 288.000, 288.000, 653.000 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 10.000 - 2.650 |
R-factor | 0.219 |
Rwork | 0.219 |
R-free | 0.21900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2ms2 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.400 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS (1.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.000 | 2.690 |
High resolution limit [Å] | 2.640 | 2.640 |
Rmerge | 0.240 | 0.395 |
Number of reflections | 175737 | |
Completeness [%] | 58.0 | 17 |
Redundancy | 1.7 | 1.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |