2A0L
Crystal structure of KvAP-33H1 Fv complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X25 |
Synchrotron site | NSLS |
Beamline | X25 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-11-10 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.1 |
Spacegroup name | P 42 2 2 |
Unit cell lengths | 136.362, 136.362, 191.812 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 57.890 - 3.900 |
R-factor | 0.358 |
Rwork | 0.358 |
R-free | 0.39200 |
Structure solution method | MIR |
RMSD bond length | 0.005 |
RMSD bond angle | 1.200 |
Data reduction software | MOSFLM |
Data scaling software | CCP4 ((SCALA)) |
Phasing software | MLPHARE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 57.700 | 4.100 |
High resolution limit [Å] | 3.900 | 3.900 |
Number of reflections | 16257 | |
<I/σ(I)> | 9.7 | 3.1 |
Completeness [%] | 97.6 | |
Redundancy | 6.94 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 293 | sodium citrate, Tric-HCl, pH 8.5, VAPOR DIFFUSION, SITTING DROP, temperature 293K |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 293 | sodium citrate, Tric-HCl, pH 8.5, VAPOR DIFFUSION, SITTING DROP, temperature 293K |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 293 | sodium citrate, Tric-HCl, pH 8.5, VAPOR DIFFUSION, SITTING DROP, temperature 293K |