271D
STRUCTURAL STUDIES ON NUCLEIC ACIDS
Experimental procedure
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1995-03-29 |
Detector | RIGAKU RAXIS IIC |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 25.427, 39.744, 65.255 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | ? - 2.020 |
R-factor | 0.176 |
Structure solution method | MIR |
RMSD bond length | 0.030 |
RMSD bond angle | 0.053 |
Data reduction software | RIGAKU |
Data scaling software | RIGAKU |
Refinement software | NUCLSQ |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 39.800 |
High resolution limit [Å] | 2.020 |
Rmerge | 0.070 |
Number of reflections | 13706 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.1 | pH 7.10 |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | ||
2 | 1 | 1 | NA CACODYLATE |