1VTI
DNA-DRUG INTERACTIONS: THE CRYSTAL STRUCTURES OF D(TGATCA) COMPLEXED WITH DAUNOMYCIN
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Temperature [K] | 275 |
| Detector technology | DIFFRACTOMETER |
| Detector | SYNTEX P21 |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 28.110, 28.110, 52.880 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 10.000 - 1.700 |
| R-factor | 0.26 |
| Refinement software | NUCLSQ |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 1.700 |
| Number of reflections | 2626 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 6.5 | 293 | pH 6.50, VAPOR DIFFUSION, temperature 293.00K |
Crystallization Reagents
| ID | crystal ID | solution ID | reagent name | concentration | details |
| 1 | 1 | 1 | WATER | 2 | 3 |
| 2 | 1 | 1 | MPD | 5 | 6 |
| 3 | 1 | 1 | MG ACETATE | 8 | 9 |
| 4 | 1 | 1 | SPERMINE_HCL | 11 | 12 |
| 5 | 1 | 1 | NA CACODYLATE | 14 | 15 |
| 6 | 1 | 2 | WATER | 17 | 18 |
| 7 | 1 | 2 | MPD | 20 | 21 |
