1UCY
THROMBIN COMPLEXED WITH FIBRINOPEPTIDE A ALPHA (RESIDUES 7-19). THREE COMPLEXES, ONE WITH EPSILON-THROMBIN AND TWO WITH ALPHA-THROMBIN
Experimental procedure
Detector technology | X1000 MULTIWIRE |
Detector | SIEMENS |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 82.470, 88.780, 98.550 |
Unit cell angles | 90.00, 106.21, 90.00 |
Refinement procedure
Resolution | 7.000 - 2.200 |
R-factor | 0.171 |
Rwork | 0.171 |
RMSD bond length | 0.011 |
RMSD bond angle | 19.400 * |
Data reduction software | XENGEN |
Data scaling software | XENGEN |
Refinement software | X-PLOR |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 7.000 | 2.300 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.072 * | |
Total number of observations | 117995 * | |
Number of reflections | 45875 | |
Completeness [%] | 15 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 8 * | Martin, P.D., (1992) J. Biol. Chem., 267, 7911. * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | ammonium sulfate | 40 (%) |