1PTR
PROTEIN KINASE C DELTA CYS2 DOMAIN COMPLEXED WITH PHORBOL-13-ACETATE
Experimental procedure
Detector technology | IMAGE PLATE |
Collection date | 1995-01-05 |
Detector | RIGAKU RAXIS IIC |
Wavelength(s) | 1.5418 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 32.400, 63.500, 65.500 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 6.000 - 2.200 |
R-factor | 0.194 |
Rwork | 0.194 |
RMSD bond length | 0.013 * |
RMSD bond angle | 3.200 |
Data reduction software | DENZO |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 2.200 |
Rmerge | 0.060 |
Number of reflections | 3215 |
Completeness [%] | 94.6 |
Redundancy | 9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 6.8 * | 4 * | used as seeds * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 8 (mg/ml) | |
2 | 1 | drop | ammonium sulfate | 55 (%) | |
3 | 1 | drop | phosphate | 0.1 (M) | |
4 | 1 | drop | DTT | 1 (mM) | |
5 | 1 | reservoir | isopropanol | 25 (%) | |
6 | 1 | reservoir | ammonium acetate | 0.2 (M) | |
7 | 1 | reservoir | sodium phosphate | 0.1 (M) |