1P1L
Structure of the Periplasmic divalent cation tolerance protein CutA from Archaeoglobus fulgidus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 110 |
Detector technology | IMAGE PLATE |
Collection date | 2003-03-12 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | I 21 3 |
Unit cell lengths | 90.967, 90.967, 90.967 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.400 - 2.000 |
R-factor | 0.2071 |
Rwork | 0.207 |
R-free | 0.22900 |
Structure solution method | SIR |
RMSD bond length | 0.007 |
RMSD bond angle | 1.200 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | CNS (0.9) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.048 | 0.118 |
Number of reflections | 8551 | |
<I/σ(I)> | 37.3 | 11 |
Completeness [%] | 93.7 | 79.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 291 | 21% PEG 1500, 0.1M Na Citrate pH 5.6, 3% MPD, 0.15M Magnesium Chloride, 0.2M Ammonium Sulfate, VAPOR DIFFUSION, HANGING DROP, temperature 291K |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 291 | 21% PEG 1500, 0.1M Na Citrate pH 5.6, 3% MPD, 0.15M Magnesium Chloride, 0.2M Ammonium Sulfate, VAPOR DIFFUSION, HANGING DROP, temperature 291K |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 291 | 21% PEG 1500, 0.1M Na Citrate pH 5.6, 3% MPD, 0.15M Magnesium Chloride, 0.2M Ammonium Sulfate, VAPOR DIFFUSION, HANGING DROP, temperature 291K |