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1OU4

Native PNP +Talo

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsCHESS BEAMLINE F1
Synchrotron siteCHESS
BeamlineF1
Temperature [K]170
Detector technologyCCD
Collection date2001-12-25
DetectorADSC QUANTUM 4
Wavelength(s)0.948
Spacegroup nameP 61 2 2
Unit cell lengths121.615, 121.615, 243.225
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution25.000

*

- 2.500
R-factor0.214
Rwork0.214
R-free0.24500

*

Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.007

*

RMSD bond angle1.350

*

Data reduction softwareMOSFLM
Data scaling softwareCCP4 ((SCALA))
Phasing softwareCNS
Refinement softwareCNS (1.0)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]25.0002.640
High resolution limit [Å]2.5002.500
Rmerge0.0760.264
Number of reflections37511

*

<I/σ(I)>7.73
Completeness [%]100.0100
Redundancy8.57.8
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP8

*

29550mM sodium Citrate, 30% ammonium sulfate, pH 5.4, VAPOR DIFFUSION, HANGING DROP, temperature 295K
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11drop10 (mM)pH8.0
21dropprotein35 (mg/ml)
31reservoirammonium sulfate30 (%)
41reservoircitrate50 (mM)pH5.4

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