1NCY
TROPONIN-C, COMPLEX WITH MANGANESE
Experimental procedure
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 66.700, 66.700, 60.800 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 8.000 - 2.100 |
| R-factor | 0.13 * |
| Rwork | 0.130 |
| RMSD bond length | 0.012 |
| RMSD bond angle | 0.046 |
| Data reduction software | PURDUE (DATA PROCESSING PACKAGE) |
| Data scaling software | PURDUE (DATA PROCESSING PACKAGE) |
| Refinement software | PROLSQ |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 8.000 |
| High resolution limit [Å] | 1.800 |
| Rmerge | 0.050 |
| Number of reflections | 29532 |
| Completeness [%] | 69.0 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | protein | 35 (mg/ml) | |
| 2 | 1 | drop | ammonium sulfate | 30 (%sat) | |
| 3 | 1 | reservoir | sodium acetate | 50 (mM) | |
| 4 | 1 | reservoir | 5 (mM) | ||
| 5 | 1 | reservoir | 1 (mM) | ||
| 6 | 1 | reservoir | ammonium sulfate | 43 (%) |
