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1LUZ

Crystal Structure of the K3L Protein From Vaccinia Virus (Wisconsin Strain)

Experimental procedure
Experimental methodMAD
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 14-BM-C
Synchrotron siteAPS
Beamline14-BM-C
Temperature [K]200
Detector technologyCCD
Collection date2000-05-01
DetectorADSC QUANTUM 4
Wavelength(s)0.9788,0.9790,1.0000
Spacegroup nameC 1 2 1
Unit cell lengths73.119, 49.580, 59.938
Unit cell angles90.00, 100.69, 90.00
Refinement procedure
Resolution500.000 - 1.800
Rwork0.232
R-free0.25600
Structure solution methodMAD
RMSD bond length0.005

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RMSD bond angle1.290

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Data reduction softwareHKL-2000
Data scaling softwareSCALEPACK
Phasing softwareSHARP
Refinement softwareCNS
Data quality characteristics
 Overall
Low resolution limit [Å]500.000
High resolution limit [Å]1.800
Rmerge0.079

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Total number of observations170730

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Number of reflections12629

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Completeness [%]99.8
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1Batch method

*

7

*

Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
111protein20 (mg/ml)
211300 (mM)
311sodium phosphate30 (mM)pH7.0
411dithiothreitol5 (mM)

221051

PDB entries from 2024-06-12

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