1LKK
HUMAN P56-LCK TYROSINE KINASE SH2 DOMAIN IN COMPLEX WITH THE PHOSPHOTYROSYL PEPTIDE AC-PTYR-GLU-GLU-ILE (PYEEI PEPTIDE)
Experimental procedure
Spacegroup name | P 21 21 21 |
Unit cell lengths | 81.840, 45.040, 26.750 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 1.000 |
R-factor | 0.133 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.700 * |
Phasing software | SHELXL-93 |
Refinement software | SHELXL-93 |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.000 * |
Rmerge | 0.070 * |
Total number of observations | 170160 * |
Number of reflections | 48786 * |
Completeness [%] | 91.0 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 7 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | SH2 domain | 35 (mg/ml) | |
2 | 1 | drop | peptide | 42 (mM) | |
3 | 1 | drop | BES | 40 (mM) |