1C47

BINDING DRIVEN STRUCTURAL CHANGES IN CRYSTALINE PHOSPHOGLUCOMUTASE ASSOCIATED WITH CHEMICAL REACTION

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Temperature [K]	289
Detector technology	IMAGE PLATE
Collection date	1996-04-01
Detector	RIGAKU RAXIS II
Spacegroup name	P 41 21 2
Unit cell lengths	174.420, 174.420, 101.100
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	6.000 - 2.700
R-factor	0.183
Rwork	0.183
R-free	0.24800
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	3pmg
RMSD bond length	0.029
RMSD bond angle	1.360
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	X-PLOR
Refinement software	X-PLOR (3.8)

Data quality characteristics

	Overall
Low resolution limit [Å]	30.000
High resolution limit [Å]	2.700
Rmerge	0.082
Number of reflections	46085
Completeness [%]	96.5
Redundancy	2.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1