1BZ7
FAB FRAGMENT FROM MURINE ASCITES
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU300 |
Temperature [K] | 300 |
Detector technology | IMAGE PLATE |
Detector | MARRESEARCH |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 146.800, 56.000, 80.000 |
Unit cell angles | 90.00, 119.20, 90.00 |
Refinement procedure
Resolution | 6.000 - 2.500 |
R-factor | 0.162 |
Rwork | 0.162 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.015 |
RMSD bond angle | 1.350 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MERLOT |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 6.000 |
High resolution limit [Å] | 2.500 |
Rmerge | 0.050 * |
Total number of observations | 79380 * |
Number of reflections | 18143 |
Completeness [%] | 94.0 |
Redundancy | 4.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 7 | used to seeding * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | zinc acetate | 0.2 (M) | |
2 | 1 | reservoir | sodium cacodylate | 0.1 (M) | |
3 | 1 | reservoir | PEG8000 | 23 (%) |