1BU7
CRYOGENIC STRUCTURE OF CYTOCHROME P450BM-3 HEME DOMAIN
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL7-1 |
Synchrotron site | SSRL |
Beamline | BL7-1 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1997-03-15 |
Detector | MARRESEARCH |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 59.380, 151.900, 62.770 |
Unit cell angles | 90.00, 96.02, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.650 |
R-factor | 0.197 |
R-free | 0.25100 |
Structure solution method | OTHER |
RMSD bond length | 0.008 |
RMSD bond angle | 0.023 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR |
Refinement software | SHELXL-97 |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 100.000 | 1.690 |
High resolution limit [Å] | 1.650 | 1.650 |
Number of reflections | 128585 | |
<I/σ(I)> | 20.6 | 5.5 |
Completeness [%] | 98.0 | 97.2 |
Redundancy | 3.4 | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 7 | unpublished data. Journal is different from PDB file. * |