1BPI

THE STRUCTURE OF BOVINE PANCREATIC TRYPSIN INHIBITOR AT 125K: DEFINITION OF CARBOXYL-TERMINAL RESIDUES GLYCINE-57 AND ALANINE-58

Experimental procedure

Temperature [K]	125
Detector technology	DIFFRACTOMETER
Collection date	1984-06
Detector	SIEMENS
Spacegroup name	P 21 21 21
Unit cell lengths	75.390, 22.581, 28.600
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 - 1.090
R-factor	0.146 *
R-free	0.21800 *
RMSD bond length	0.035 *
RMSD bond angle	3.100 *
Data reduction software	XFIT
Phasing software	SHELXL-93
Refinement software	SHELXL-93

Data quality characteristics

	Overall
Total number of observations	28980 *
Number of reflections	20781 *
Completeness [%]	99.9 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion *	10 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	50 (mg/ml)
2	1	drop	K-Na phosphate	0.5 (M)
3	1	reservoir	K-Na phosphate	0.5 (M)