1AYL
PHOSPHOENOLPYRUVATE CARBOXYKINASE
Experimental procedure
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-6B |
Synchrotron site | Photon Factory |
Beamline | BL-6B |
Detector technology | IMAGE PLATE |
Detector | FUJI |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 127.510, 96.690, 46.960 |
Unit cell angles | 90.00, 96.63, 90.00 |
Refinement procedure
Resolution | 6.000 - 1.800 |
R-factor | 0.195 |
Rwork | 0.195 |
R-free | 0.23400 |
RMSD bond length | 0.005 |
RMSD bond angle | 24.400 * |
Data reduction software | WEIS |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.800 * |
Rmerge | 0.076 |
Number of reflections | 40067 |
Completeness [%] | 76.7 |
Redundancy | 2.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 4.4 * | 21 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | PCK | 8 (mg/ml) | |
10 | 1 | reservoir | ammonium acetate | 200 (mM) | |
11 | 1 | reservoir | PEG4000 | 27 (%(w/v)) | |
2 | 1 | drop | ATP | 2 (mM) | |
3 | 1 | drop | oxalate | 2 (mM) | |
4 | 1 | drop | 5 (mM) | ||
5 | 1 | drop | EDTA | 1 (mM) | |
6 | 1 | drop | sodium acetate | 100 (mM) | |
7 | 1 | drop | ammonium acetate | 200 (mM) | |
8 | 1 | drop | PEG4000 | 12 (%(w/v)) | |
9 | 1 | reservoir | sodium acetate | 100 (mM) |