1AUY
TURNIP YELLOW MOSAIC VIRUS
Experimental procedure
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X12C |
Synchrotron site | NSLS |
Beamline | X12C |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE AREA DETECTOR |
Collection date | 1994-10 |
Detector | MARRESEARCH |
Spacegroup name | P 64 2 2 |
Unit cell lengths | 515.500, 515.500, 309.500 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 8.000 - 3.000 |
R-factor | 0.187 |
Rwork | 0.187 |
R-free | 0.19300 |
Structure solution method | MOLECULAR REPLACEMENT/MULTIPLE ISOMORPHOUS REPLACEMENT |
Starting model (for MR) | COWPEA CHLOROTIC MOTTLE VIRUS (CCMV) |
RMSD bond length | 0.013 |
RMSD bond angle | 27.500 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASES |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.180 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.105 * | 0.103 |
Number of reflections | 348694 | |
Completeness [%] | 73.7 | 4.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 3.7 | 25 * | 1.11 M AMMONIUM PHOSPHATE 100 MM MES PH 3.7 HANGING DROP, vapor diffusion - hanging drop |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | ammonium phosphate | 1.11-1.15 (M) | |
2 | 1 | reservoir | MES | 100 (mM) |