1AF6
MALTOPORIN SUCROSE COMPLEX
Experimental procedure
Source type | SYNCHROTRON |
Source details | SRS BEAMLINE PX9.6 |
Synchrotron site | SRS |
Beamline | PX9.6 |
Temperature [K] | 293 |
Detector technology | IMAGE PLATE |
Collection date | 1995-05-12 |
Detector | MARRESEARCH |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 129.660, 211.510, 217.910 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.400 |
R-factor | 0.195 * |
Rwork | 0.195 |
R-free | 0.21400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1mal |
RMSD bond length | 0.009 |
RMSD bond angle | 0.021 |
Data reduction software | MOSFLM |
Data scaling software | CCP4 ((ROTAVATA)) |
Phasing software | CCP4 |
Refinement software | PROLSQ |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.460 |
High resolution limit [Å] | 2.400 | 2.360 |
Rmerge | 0.065 | 0.350 |
Number of reflections | 114378 | |
<I/σ(I)> | 5.7 | 2 |
Completeness [%] | 99.0 | 98.8 |
Redundancy | 3.8 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 7 | pH 7. |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | beta-D-decylmaltoside | 0.4 (%(w/w)) | |
2 | 1 | 1 | HEPES | 20 (mM) | |
3 | 1 | 1 | 0.1 (0.1) | ||
4 | 1 | 1 | PEG2000 | 11.0-12.5 (%(w/w)) |