8CGT
STRUCTURE OF CYCLODEXTRIN GLYCOSYLTRANSFERASE COMPLEXED WITH A THIO-MALTOHEXAOSE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 298 |
Detector technology | AREA DETECTOR |
Collection date | 1996-11-01 |
Detector | SIEMENS |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 94.400, 104.900, 113.700 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 2.400 |
R-factor | 0.157 |
Rwork | 0.157 |
R-free | 0.17800 |
Structure solution method | OTHER |
RMSD bond length | 0.010 |
RMSD bond angle | 1.300 |
Data reduction software | XDS |
Data scaling software | XDS |
Refinement software | X-PLOR (3.851) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.317 | 2.260 |
High resolution limit [Å] | 2.200 | 2.200 |
Number of reflections | 48544 | |
<I/σ(I)> | 15.1 | 4.3 |
Completeness [%] | 84.2 | 51.9 |
Redundancy | 3.2 | 1.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.9 | pH 6.9 |