6KBX
Crystal structure of yedK in complex with ssDNA containing abasic site
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-01-08 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.979 |
Spacegroup name | P 1 21 1 |
格子定数 [Å] | 47.092, 44.084, 54.731 |
格子定数 [度] | 90.00, 101.69, 90.00 |
精密化法
残基 | 46.115 - 1.221 |
R因子 | 0.1557 |
Rwork | 0.155 |
R-free | 0.16470 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6kbs |
結合長の平均二乗偏差(RMSD) [Å] | 0.005 |
結合角の平均二乗偏差(RMSD) [度] | 0.920 |
Data reduction software | HKL-3000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (1.12_2829) |
Quality characteristics
Overall | Inner shell | Outer shell | |
分解能 [Å] (低) | 50.000 | 50.000 | 1.260 |
分解能 [Å] (高) | 1.220 | 2.630 | 1.220 |
Rmerge_l_obs | 0.091 | 0.065 | 0.619 |
Rmeas | 0.098 | 0.071 | 0.691 |
Rpim | 0.038 | 0.027 | 0.299 |
Total number of observations | 416830 | ||
独立反射数 | 64468 | 6663 | 6072 |
<I/σ(I)> | 5.1 | ||
完全性 [%] | 98.8 | 99.5 | 93.6 |
冗長性 | 6.5 | 6.8 | 4.6 |
CC(1/2) | 0.995 | 0.676 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | EVAPORATION | 293 | 0.2 M sodium formate, 20% PEG3350 |