6J8F
Crystal structure of SVBP-VASH1 with peptide mimic the C-terminal of alpha-tubulin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-10-21 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9792 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 66.950, 108.377, 46.896 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 54.188 - 2.283 |
R-factor | 0.2015 |
Rwork | 0.200 |
R-free | 0.23690 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | low resolution SeMet structure |
RMSD bond length | 0.003 |
RMSD bond angle | 0.685 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX ((1.14_3260: ???)) |
Refinement software | PHENIX ((1.14_3260: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 54.190 | 2.410 |
High resolution limit [Å] | 2.280 | 2.280 |
Rpim | 0.491 | |
Number of reflections | 16147 | 2322 |
<I/σ(I)> | 10.9 | 2.2 |
Completeness [%] | 99.9 | 100 |
Redundancy | 12.5 | 12.9 |
CC(1/2) | 0.726 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.1M Na citrate tribasic dihydrate pH 5.0, 18% PEG 20000 |